Analytical Method Development and Stability Studies of by Kishanta Kumar Pradhan,Ranganadha Rao K,P. Srinivasulu PDF

By Kishanta Kumar Pradhan,Ranganadha Rao K,P. Srinivasulu

Master's Thesis from the 12 months 2011 within the topic medication - Pharmacology, grade: 8.0, , direction: B.Pharm.,M.Pharm, language: English, summary: A opposite part excessive functionality liquid chromatographic technique (HPLC) has been constructed for the strategy improvement validation of Carvedilol in bulk and pharmaceutical formula by utilizing YMC PACK seasoned 4.6 X one hundred fifty mm (5µm Particle size). The cellular section was once Buffer: Acetonitrile: (70:30) and pH was once adjusted to two pumped at a stream cost of one ml/min and the eluents have been monitored at 320nm. Linearity used to be received within the focus diversity of 10-90 μg/ml. The retention time of Carvedilol was once chanced on to be 3.2 minute. the strategy used to be verified for specificity, accuracy, precision, linearity, and restrict of detection, restrict of quantification, robustness and solubility balance. LOD and LOQ have been came upon to be 0.001 μg/ml and 0.011μg/ml respectively. the tactic used to be statistically confirmed and RSD used to be came upon to be under 2% indicating excessive measure of accuracy and precision of the proposed HPLC technique. balance research record published that the drug is weak for acidic, alkaline, oxidative, photolytic and UV degradation. The drug is strong to thermal degradation. extra over the degradants have been good separated from its API. because of its simplicity, rapidness, excessive precision and accuracy, the proposed HPLC technique can be used for picking Carvedilol in bulk drug samples or in pharmaceutical dosage forms.

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Analytical Method Development and Stability Studies of Carvedilol by Kishanta Kumar Pradhan,Ranganadha Rao K,P. Srinivasulu

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